DMF is hydrolyzed by strong acids and bases, especially at elevated temperatures. With sodium hydroxide, DMF converts to formate and dimethylamine. DMF undergoes decarbonylation near its boiling point to give dimethylamine.US $2,030
30+ Tons
CAS No.: | 68-12-2 |
---|---|
Formula: | Hcon(CH3)2 |
EINECS: | 200-679-5 |
Type: | Synthesis Material Intermediates |
Appearance: | Liquid |
Quality: | Industrial |
Dimethyl Formamide/DMF with Cheap Price CAS No 68-12-2
Dimethylformamide is an organic compound with the formula (CH3)2NC(O)H. Commonly abbreviated as DMF (although this initialism is sometimes used for dimethylfuran, or dimethyl fumarate), this colourless liquid is miscible with water and the majority of organic liquids. DMF is a common solvent for chemical reactions. Dimethylformamide is odorless, but technical-grade or degraded samples often have a fishy smell due to impurity of dimethylamine. Dimethylamine degradation impurities can be removed by sparging degraded samples with an inert gas such as argon or by sonicating the samples under reduced pressure. As its name indicates, it is a derivative of formamide, the amide of formic acid. DMF is a polar (hydrophilic) aprotic solvent with a high boiling point. It facilitates reactions that follow polar mechanisms, such as SN2 reactions.
DMF is hydrolyzed by strong acids and bases, especially at elevated temperatures. With sodium hydroxide, DMF converts to formate and dimethylamine. DMF undergoes decarbonylation near its boiling point to give dimethylamine. Distillation is therefore conducted under reduced pressure at lower temperatures.
In one of its main uses in organic synthesis, DMF was a reagent in the Vilsmeier-Haack reaction, which is used to formylate aromatic compounds.The process involves initial conversion of DMF to a chloroiminium ion, [(CH3)2N=CH(Cl)]+, known as a Vilsmeier reagent, which attacks arenes.
Organolithium compounds and Grignard reagents react with DMF to give aldehydes after hydrolysis in a reaction named after Bouveault.
Dimethylformamide forms 1:1 adducts with a variety of Lewis acids such as the soft acid I2, and the hard acid phenol. It is classified as a hard Lewis base and its ECW model base parameters are EB= 2.19 and CB= 1.31.[17] Its relative donor strength toward a series of acids, versus other Lewis bases, can be illustrated by C-B plots.
ITEM | SPECIFICATION | RESULTS |
Pt-Co chrominance | ≤10 | 5 |
Dimethylamine ppm | ≤15 | 1 |
Formic acid ppm | ≤25 | 2 |
PH: 25°C 20%Aqueous solution | 6.5-8.0 | 7.0 |
Electric Conductivity: 25°C 20%Aqueous solution, us | ≤10 | 0.14 |
Moisture ppm | ≤500 | 106 |
Fe ppm | ≤0.05 | 0.005 |
Methanel ppm | ≤20 | 2 |
Heavy compoment (dimethyl Acetamide) ppm | ≤500 | 39 |
DMF % | ≥99.9 | 99.95 |
The primary use of DMF is as a solvent with low evaporation rate. DMF is used in the production of acrylic fibers and plastics. It is also used as a solvent in peptide coupling for pharmaceuticals, in the development and production of pesticides, and in the manufacture of adhesives, synthetic leathers, fibers, films, and surface coatings.
As a cheap and common reagent, DMF has many uses in a research laboratory.
We have various of packages for different products and we are always pleased to satisfy customers' request.
Packaging:
190kg*80 drums,15.2ton/20'FCL;
190kg*132 drums,25.08ton/40'FCL;
22ton/ISO TANK.
Shipping:
Promote shipping usually 7--14 days after receiving TT deposit or LC Original .
1 Q:Are you manufacturer?
A: As an integrated enterprise, we have our own production lines on Methylene Chloride, Chloroform and Aniline oil, meanwhile we are one of the experienced distributors for other chemicals such as cyclohexanone, Dimethyl Formamide, Propylene Glycol, Ethylene Glycol, Dimethyl Carbonate, Thiourea, Polyol, TDI, IPA, Ethanol etc. We have competitive price benefited by ready stock and good relations with some leading chemical manufacturers.
2 Q: How can you guarantee your quality?
A: Our factory owns mature production line under EPR quality system. We can guarantee the stability and qualification of the raw materials. And we also have SOP loading system to ensure the safety and timely transportation.
3 Q: Can I get some samples?
A: Yes, we welcome sample order for you to test and check our quality. Send me your requirements of the product you need. We can provide sample free of charge, and the express cost is on you.
4 Q: How to confirm the Product Quality before placing orders?
A : You can get free samples from us or taking our previous SGS Reports as reference or arrange SGS before loading.
5 Q: What is your MOQ?
A: Our MOQ is 20'FCL for each product.
6 Q: What kind of package do you have?
A: We have various of packages to meet needs of our customers,like Iron drums,plastic drums, IBC tanks, Flexitank, ISO TANK and bags etc.
7 Q :Which kind of payment terms do you accept?
A: TT, LC, payment terms are acceptable.
8 Q:Can you give me a discount price?
A: Yes. It depends on your order qty.
9 Q: How about your delivery? How long is your delivery time?
A: Prompt and reliable delivery by professional shipping lines.
Generally it takes 14 days after deposit or original LC.
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